Basic instrumental analysis
Informacje ogólne
Kod przedmiotu: | 7-D-SK.EN-09 |
Kod Erasmus / ISCED: |
(brak danych)
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(0531) Chemia
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Nazwa przedmiotu: | Basic instrumental analysis |
Jednostka: | Instytut Chemii |
Grupy: |
Katalog przedmiotów dla studiów krótkoterminowych (Erasmus+ lub inne umowy o współpracy) Kursy zmienne ogólnouczelniane prowadzone w języku obcym nowożytnym |
Punkty ECTS i inne: |
(brak)
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Język prowadzenia: | angielski |
Tryb prowadzenia: | Lektura monograficzna |
Skrócony opis: |
(tylko po angielsku) 1. Principles of instrumental chemical analysis that includes optical spectroscopy, electroanalytical techniques, chromatography, and selected spectroscopy techniques. 2. Gain understanding in the application of these techniques to evaluate data to answer qualitative and quantitative questions about a chemical sample |
Pełny opis: |
(tylko po angielsku) Lecture Topics 1.INTRODUCTION (Statistics, Signals and Noise) 2. OPTICAL SPECTROSCOPY (refractometry, polarymetry, nephelometry) 3. ELECTROCHEMICAL METHODS (Electrochemical concepts, potentiometry, conductometry, coulometry, Voltametry, polarography) 4.MOLECULAR SPECTROSCOPY(UV/VIS, IR, NMR) 5.ATOMIC SPECTROSCOPY(Properties of Light, Instrumentation, and Sources, Absorption, Emission) 6.MASS SPECTROMETRY(Instrumentation, elemental & molecular, Ionization methods) 7.SEPARATIONS TECHNIQUES (Chromatography (GC, LC), Electrophoresis, Instrumentation) Laboratory issues: - getting familiar with the apparatus, its use and independent analysis and preparation of results. - Performing experiments in the field of potentiometric and pH measurements, refractometry, conductometry, amperometry, nephelometry and turbidimetry, polarymetry and spectrophotometric UV-VIS. - Separation of organic compounds by means of high performance liquid chromatography (HPLC. Spectroscopic determination of the content of various analytes in natural samples. |
Literatura: |
(tylko po angielsku) A. Skoog, F. J. Holler, and S. R. Crouch, Principles of Instrumental Analysis, 7thEdition. |
Efekty uczenia się: |
(tylko po angielsku) Specific Course Learning Objectives Include:*Demonstrate knowledge of sampling methods for all states of matter. *Assess sources of error in chemical and instrumental analysis and account for errors in data analysis. *Recognize interferences in chemical and instrumental analysis. *Comprehend the concept of and perform instrument and method calibration. *Apply and assess concepts of availability and evaluation of analytical standards and formulate standardization methodology. *Integrate a fundamental understanding of the underlining physics principles as they relate to specific instrumentation used for atomic, molecular, and mass spectrometry, magnetic resonance spectrometry and chromatography. *Understand and be able to apply the theory and operational principles of analytical instruments. *Distinguish between qualitative and quantitative measurements and be able to effectively compare and critically select methods for elemental and molecular analyses. |
Metody i kryteria oceniania: |
(tylko po angielsku) • short tests with open questions • practical tests • laboratory notes --> Obligatory participation in laboratory. --> Lab reports:There are 7 laboratories, you will turn in 7 individual lab reports. The grade is based on lab pre-write-ups, lab reports, and lab notebook. --> Final exam at the end of the semester |
Praktyki zawodowe: |
(tylko po angielsku) ✔ Practical and/or problem-solving skills ✔ Specialist skills |
Właścicielem praw autorskich jest Uniwersytet Opolski.